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1 article(s) from Andersen, Sissel S

Advances in the synthesis of functionalised pyrrolotetrathiafulvalenes

Luke J. O’Driscoll,
Sissel S. Andersen,
Marta V. Solano,
Dan Bendixen,
Morten Jensen,
Troels Duedal,
Jess Lycoops,
Cornelia van der Pol,
Rebecca E. Sørensen,
Karina R. Larsen,
Kenneth Myntman,
Christian Henriksen,
Stinne W. Hansen and
Jan O. Jeppesen

Beilstein J. Org. Chem. 2015, 11, 1112–1122, doi:10.3762/bjoc.11.125

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Figure 1: The sequential, reversible oxidation of TTF (1) to its stable radical cation (2) and dication (3) s...

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Figure 2: Structures and possible substitution positions of MPTTFs (4) and BPTTFs (5).

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Scheme 1: Large-scale synthesis of 6. Reagents and conditions: a) PhMe, reflux, 19 h, 74%; b) LiBr, NaBH₄, TH...

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Scheme 2: Preparation of 7. Reagents and conditions: a) TsCl, Et₃N, DMAP, MeCN, rt → reflux, 3.5 h, 82%; b) (...

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Scheme 3: Homo and cross-coupling reactions of 6 or 7 afford BPTTFs and MPTTFs, respectively. Reagents and co...

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Scheme 4: Deprotection and methylation of cyanoethyl-protected thiol moieties on MPTTFs as reported by Jeppes...

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Scheme 5: Deprotection and alkylation of cyanoethyl-protected thiol moieties on MPTTFs using CsOH·H₂O or DBU....

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Scheme 6: Deprotection and N-arylation of tosylated MPTTFs. Reagents and conditions: a) NaOMe, THF, MeOH, ref...

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Scheme 7: Deprotection and N,N-diarylation of tosylated BPTTFs. Reagents and conditions: a) NaOMe, THF, MeOH,...

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Published 03 Jul 2015

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